2,2-dimethyl-3,4-dihydronaphthalen-1-one synthesis
- Product Name:2,2-dimethyl-3,4-dihydronaphthalen-1-one
- CAS Number:2977-45-9
- Molecular formula:C12H14O
- Molecular Weight:174.24
26059-40-5
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2977-45-9
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$24.00/250mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: Et3N / CH2Cl2 / 0 - 20 °C
2.1: NaI / acetone / Heating
3.1: n-BuLi; i-Pr2NH / hexane; tetrahydrofuran / 1 h / -78 °C
3.2: tetrahydrofuran; hexane / -78 - 20 °C
4.1: 69 percent Spectr. / PPh3; Et3N / Pd(OAc)2 / dimethylformamide; H2O / 24 h / 130 °C
References:
Pletnev, Alexandre A.;Larock, Richard C. [Journal of Organic Chemistry,2002,vol. 67,# 26,p. 9428 - 9438]
529-34-0
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74-88-4
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2977-45-9
48 suppliers
$24.00/250mg
1590-08-5
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$36.00/1g
74-88-4
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2977-45-9
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$24.00/250mg
4374-44-1
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2977-45-9
48 suppliers
$24.00/250mg
530-93-8
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$10.00/1g
74-88-4
353 suppliers
$15.00/10g
2977-45-9
48 suppliers
$24.00/250mg