2,3,3-TRIMETHYLHEXANE synthesis

5synthesis methods

Product Name:2,3,3-TRIMETHYLHEXANE
CAS Number:16747-28-7
Molecular formula:C9H20
Molecular Weight:128.26

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Yield:-

Reaction Conditions:

at 20; under 760.051 Torr;Gas phase;

Steps:

2 Example 2
A device of FIGS. 1 and 3-8 and as provided herein was operated at the following parameters: 440 Hz; 24,600 VAC sec voltage; atmospheric pressure; and ambient temperature. The gas phase hydrocarbon input was propane. Four (4) samples were collected. Sample 1 was a solvent blank containing only acetone. Sample 2 was solid residue collected from the reactor wall, diluted. Sample 3 was liquid product stream, diluted. Sample 4 was neat liquid product stream. Descriptions of samples S1 to S4 are provided in Table 2. Gas chromatography was performed using an Agilent HP-5 column, having a 30 m length, a 0.25 mm inner diameter and a split ratio of 50:1. The temperature program was as follows: temperature was held at 40° C. for 3 min; 40-200° C. at a heating rate of 5° C./min; then 200-280° C. at a heating rate of 10° C./min. Mass spectrometry results for sample S4, using a best fit model, are provided in Table 3. Gas chromatography results for sample S4 are provided in Table 4.

References:

PlasMerica, LLC US2021/32183, 2021, A1 Location in patent:Paragraph 0176-0178