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40358-33-6

2,3,4,5-TETRAHYDRO-1,5-BENZOTHIAZEPINE synthesis

7synthesis methods
15857-68-8 Synthesis
2,3-dihydro-4H-1-benzothiopyran-4-one oxime

15857-68-8
16 suppliers
$28.60/250mg

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Yield:40358-33-6 76%

Reaction Conditions:

with dichloroaluminum hydride in cyclopentyl methyl ether at 0 - 20; for 2.25 h;

References:

Cho, Hidetsura;Iwama, Yusuke;Mitsuhashi, Nakako;Sugimoto, Kenji;Okano, Kentaro;Tokuyama, Hidetoshi [Molecules,2012,vol. 17,# 6,p. 7348 - 7355] Location in patent:experimental part