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ChemicalBook CAS DataBase List 2,3,5,6-TETRACHLOROBENZENE-1-THIOL
4707-16-8

2,3,5,6-TETRACHLOROBENZENE-1-THIOL synthesis

5synthesis methods
-

Yield:4707-16-8 64%

Reaction Conditions:

with sulfur;1,10-Phenanthroline;copper dichloride;sodium t-butanolate in N,N-dimethyl-formamide at 25; for 12 h;Schlenk technique;Inert atmosphere;

References:

Yan, Haiming;Huang, Zhiliang;Chen, Meng;Li, Cuiting;Chen, Ya;Gao, Meng;Lei, Aiwen [Organic and Biomolecular Chemistry,2017,vol. 15,# 39,p. 8276 - 8279] Location in patent:supporting information

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