2,3-DIHYDROXY-5-METHYL-BENZOIC ACID synthesis
- Product Name:2,3-DIHYDROXY-5-METHYL-BENZOIC ACID
- CAS Number:6049-93-0
- Molecular formula:C8H8O4
- Molecular Weight:168.15
4386-42-9
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6049-93-0
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$72.00/100mg
Yield:6049-93-0 87%
Reaction Conditions:
Stage #1: 2-hydroxy-3-methoxy-5-methylbenzoic acidwith boron tribromide in dichloromethane at -78 - 20;Inert atmosphere;
Stage #2: with methanol in dichloromethane at 20;Inert atmosphere;
References:
Lang, Yunhui;Souza, Fabio E. S.;Xu, Xinshe;Taylor, Nicholas J.;Assoud, Abdeljalil;Rodrigo, Russell [Journal of Organic Chemistry,2009,vol. 74,# 15,p. 5429 - 5439] Location in patent:supporting information; experimental part
93-51-6
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$15.00/5g
6049-93-0
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$72.00/100mg
17746-75-7
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6049-93-0
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89-56-5
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$11.00/5g
6049-93-0
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$72.00/100mg
124-38-9
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$214.00/14L
452-86-8
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$5.00/5g
6049-93-0
24 suppliers
$72.00/100mg