2-(4-AMINO-PHENOXY)-ACETAMIDE synthesis
- Product Name:2-(4-AMINO-PHENOXY)-ACETAMIDE
- CAS Number:58232-55-6
- Molecular formula:C8H10N2O2
- Molecular Weight:166.18
63218-14-4
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Yield:58232-55-6 100%
Reaction Conditions:
with palladium 10% on activated carbon;hydrogen;Sodium sulfate [anhydrous] in methanol; under 2585.81 Torr; for 2 h;
Steps:
7.3.443 7.3.443 N2,N4-Bis[4-(aminocarbonylmethyleneoxy)phenyl]-5-fluoro-2,4-pyrimidinediamine (R945025)
Hydrogenation of 1-aminocarbonylmethyleneoxy-4-nitrobenzene (3 g, 15 mmol) in methanol (50 mL) catalyzed by 10% Pd-C (500 mg) and Na2SO4 (500 mg) at 50 psi for 2 h gave 4-(aminocarbonylmethyleneoxy)aniline (2.59 g, quant.).
References:
US2015/266828,2015,A1 Location in patent:Paragraph 1000
100-02-7
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58232-55-6
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59954-04-0
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58232-55-6
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694454-63-2
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![Acetic acid, 2-[4-[[(phenylmethoxy)carbonyl]amino]phenoxy]-](/CAS/20210305/GIF/166383-74-0.gif)
166383-74-0
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58232-55-6
25 suppliers
$85.00/250mg