2-(4-methoxy-2-(trifluoromethyl)phenyl)acetic acid synthesis
- Product Name:2-(4-methoxy-2-(trifluoromethyl)phenyl)acetic acid
- CAS Number:916420-90-1
- Molecular formula:C10H9F3O3
- Molecular Weight:234.17
124-38-9
129 suppliers
$214.00/14L
916420-86-5
13 suppliers
$94.29/1g
916420-90-1
16 suppliers
$128.00/1g
Yield:916420-90-1 43%
Reaction Conditions:
Stage #1: carbon dioxide;4-methoxy-2-(trifluoromethyl)benzyl bromidewith N,N,N,N,-tetramethylethylenediamine;1,3-dicyano-2,4,5,6-tetrakis(N,N-diphenylamino)-benzene;Cs2CO3 in N,N-dimethyl-formamide at 20; under 760.051 Torr; for 16 h;Irradiation;
Stage #2: Acidic conditions;
References:
Jing, Ke;Wei, Ming-Kai;Yan, Si-Shun;Liao, Li-Li;Niu, Ya-Nan;Luo, Shu-Ping;Yu, Bo;Yu, Da-Gang [Cuihua Xuebao/Chinese Journal of Catalysis,2022,vol. 43,# 7,p. 1667 - 1673]