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79623-15-7

2-(4-methoxyphenyl)-tetrahydrofuran synthesis

11synthesis methods
-

Yield:79623-15-7 93.2%

Reaction Conditions:

Stage #1: para-iodoanisolewith iodine;magnesium in tetrahydrofuran at 0 - 20;Inert atmosphere;
Stage #2: tetrahydrofuranwith iron(III) oxide at 0 - 20; for 6 h;Inert atmosphere;

References:

Singh, Parvinder Pal;Gudup, Satish;Ambala, Srinivas;Singh, Umed;Dadhwal, Sumit;Singh, Baldev;Sawant, Sanghapal D.;Vishwakarma, Ram A. [Chemical Communications,2011,vol. 47,# 20,p. 5852 - 5854] Location in patent:supporting information; experimental part