2-[(4-METHYLBENZYL)SULFANYL]BENZENECARBOXYLIC ACID synthesis
- Product Name:2-[(4-METHYLBENZYL)SULFANYL]BENZENECARBOXYLIC ACID
- CAS Number:104351-51-1
- Molecular formula:C15H14O2S
- Molecular Weight:258.34
104-81-4
198 suppliers
$17.00/5g
147-93-3
433 suppliers
$7.00/5g
104351-51-1
26 suppliers
$115.00/500mg
Yield:104351-51-1 91%
Reaction Conditions:
Stage #1: Thiosalicylic acidwith sodium hydroxide in methanol at 25; for 0.5 h;
Stage #2: 4-Methylbenzyl bromide in acetone; for 4 h;Reflux;
Stage #3: with hydrogenchloride in methanol;water;
References:
Porter, Brianne L.;McClure, Beth Anne;Abrams, Eric R.;Engle, James T.;Ziegler, Christopher J.;Rack, Jeffrey J. [Journal of Photochemistry and Photobiology A: Chemistry,2011,vol. 217,# 2-3,p. 341 - 346] Location in patent:experimental part