
2,5-DIETHYL-4-IODO-BENZOIC ACID synthesis
- Product Name:2,5-DIETHYL-4-IODO-BENZOIC ACID
- CAS Number:100127-56-8
- Molecular formula:C11H13IO2
- Molecular Weight:304.1242
Yield:100127-56-8 57%
Reaction Conditions:
Stage #1: 1,4-diiodo-2,5-diethylbenzenewith n-butyllithium in tetrahydrofuran;hexane at -78; for 1.66667 h;
Stage #2: carbon dioxide in tetrahydrofuran;hexane at -78 - 20;
References:
Jian, Huahua;Tour, James M. [Journal of Organic Chemistry,2005,vol. 70,# 9,p. 3396 - 3424]

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