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100127-56-8

2,5-DIETHYL-4-IODO-BENZOIC ACID synthesis

2synthesis methods
-

Yield:100127-56-8 57%

Reaction Conditions:

Stage #1: 1,4-diiodo-2,5-diethylbenzenewith n-butyllithium in tetrahydrofuran;hexane at -78; for 1.66667 h;
Stage #2: carbon dioxide in tetrahydrofuran;hexane at -78 - 20;

References:

Jian, Huahua;Tour, James M. [Journal of Organic Chemistry,2005,vol. 70,# 9,p. 3396 - 3424]

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