2,6-dimethoxy-3-(trimethylsilyl)pyridine synthesis
- Product Name:2,6-dimethoxy-3-(trimethylsilyl)pyridine
- CAS Number:1373693-69-6
- Molecular formula:C10H17NO2Si
- Molecular Weight:211.33
Yield:1373693-69-6 69%
Reaction Conditions:
Stage #1: 3-bromo-2,6-dimethoxypyridinewith n-butyllithium;isopropylmagnesium chloride in tetrahydrofuran;hexane at -2 - 0; for 0.75 h;Inert atmosphere;
Stage #2: chloro-trimethyl-silane in tetrahydrofuran;hexane at 0 - 20;Inert atmosphere;
References:
Struk, Lukasz;Sosnicki, Jacek G. [Synthesis,2012,vol. 44,# 5,p. 735 - 746] Location in patent:experimental part
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