2-amino-2-phenyl-1-(piperidin-1-yl)ethan-1-one synthesis
- Product Name:2-amino-2-phenyl-1-(piperidin-1-yl)ethan-1-one
- CAS Number:24153-06-8
- Molecular formula:C13H18N2O
- Molecular Weight:218.29
110-89-4
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 20 °C / Inert atmosphere
1.2: 3 h / 0 - 20 °C / Inert atmosphere
2.1: ammonium salicylate; titanium isopropoxide; hydrogen; [Ru(OAc)2(rac-2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl)] / 2,2,2-trifluoroethanol / 24 h / 80 °C / 38002.6 Torr / Autoclave
References:
Hu, Le'an;Wang, Yuan-Zheng;Xu, Lei;Yin, Qin;Zhang, Xumu [Angewandte Chemie - International Edition,2022,vol. 61,# 25,art. no. E202202552][Angew. Chem.,2022,vol. 134,# 25]
14377-63-0
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611-73-4
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