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2-azido-1,3,5-trichlorobenzene synthesis

1synthesis methods
-

Yield:61371-35-5 95%

Reaction Conditions:

with sodium azide;sulfuric acid;sodium nitrite1.) 40 degC, 2.) water, acetic acid, 60 degC;

References:

Onys'ko, P. P.;Proklina, N. V.;Prokopenko, V. P.;Gololobov, Yu. G. [Journal of general chemistry of the USSR,1984,vol. 54,# 2,p. 289 - 296][Zhurnal Obshchei Khimii,1984,vol. 54,# 2,p. 325 - 333]