2,4,6-Trichloroaniline synthesis
- Product Name:2,4,6-Trichloroaniline
- CAS Number:634-93-5
- Molecular formula:C6H4Cl3N
- Molecular Weight:196.46
Process for the preparation of 2,4,6-trichloroaniline
18708-70-8
114 suppliers
$12.00/1g
634-93-5
222 suppliers
$12.00/5g
Yield:634-93-5 97%
Reaction Conditions:
with hydrazine hydrate monohydrate in N,N-dimethyl-formamide at 100; for 6 h;Green chemistry;chemoselective reaction;
Steps:
Synthesis of amines; general procedure
General procedure: A mixture of the organic nitro compound (1.0 mmol), NH2NH2·H2O (2.5 equiv.) and H2O2-treated AC powder (50 wt%) in DMF (1.5 mL) was stirred vigorously magnetically at 100 °C. The reaction was monitored by LC-MS or GC-MS. On completion the reaction mixture was filtered to remove the catalyst. The combined organic mixture material was dried using anhydrous Na2SO4 and filtered. The solvent was removed under reduced pressure to obtain the products. All the compounds were known and characterised by their 1H NMR and MS spectra and comparison with literature data.
References:
Jiang, Yuqin;Suo, Huajun;Zhang, Dandan;Li, Xiyong;Sun, Yamin;Ren, Baoqi;Zhang, Weiwei;Xu, Guiqing [Journal of Chemical Research,2017,vol. 41,# 9,p. 509 - 512]
62-53-3
691 suppliers
$10.00/1g
634-93-5
222 suppliers
$12.00/5g
142-04-1
208 suppliers
$10.00/10g
634-93-5
222 suppliers
$12.00/5g
106-47-8
486 suppliers
$5.00/5G
634-93-5
222 suppliers
$12.00/5g
95-51-2
390 suppliers
$5.00/5G
634-93-5
222 suppliers
$12.00/5g