2-broMo-4-iodo-6-nitro-aniline synthesis

3synthesis methods

Product Name:2-broMo-4-iodo-6-nitro-aniline
CAS Number:873980-29-1
Molecular formula:C6H4BrIN2O2
Molecular Weight:342.92

59255-95-7 Synthesis

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Yield:873980-29-1 9 g

Reaction Conditions:

with N-iodo-succinimide in acetic acid at 50;

Steps:

1.2 Step 2:2 - bromo -4 - iodo -6 - nitroaniline

The 2 - bromo -6 - nitroaniline (5.65 g, 26.0 mmol) is dissolved in acetic acid (40 ml), then add N - iodo succinimide (5.4 g, 31.2 mmol), the reaction liquid 50 °C stirring overnight, then cooled to room temperature. Water and dilute the reaction liquid, continuing to stir 10 minutes. Filtered to obtain the title compound crude product (9 g), as an orange solid.

References:

CN108314680,2018,A Location in patent:Paragraph 0358; 0359; 0363-0365

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References

88-74-4 Synthesis

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References