2-Bromo-N-methylacetanilide synthesis
- Product Name:2-Bromo-N-methylacetanilide
- CAS Number:29182-97-6
- Molecular formula:C9H10BrNO
- Molecular Weight:228.09
598-21-0
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$10.00/10g
100-61-8
406 suppliers
$8.00/1g
29182-97-6
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$45.00/50mg
Yield:29182-97-6 100%
Reaction Conditions:
with triethylamine in ethyl acetate at 0 - 25; for 0.5 h;
Steps:
33
Reference Example 33 2-Bromo-N-methyl-N-phenylacetamide To a solution of N-methylaniline (1.90 mL, 17.5 mmol) and triethylamine (2.44 mL, 17.5 mmol) in ethyl acetate (40 mL) is added a solution of bromoacetyl bromide (1.52 mL, 17.5 mmol) in ethyl acetate (40 mL) at 0°C, and the mixture is stirred at 20-25°C for 30 minutes. After the reaction, the mixture is filtered, and the solvent is evaporated under reduced pressure to give 2-bromo-N-methyl-N-phenylacetamide (4.60 g, quantitative). IR (cm-1): 1109, 1375, 1593, 1624, 1683
References:
EP1719761,2006,A1 Location in patent:Page/Page column 33
13094-51-4
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$90.00/50mg
100-61-8
406 suppliers
$8.00/1g
29182-97-6
49 suppliers
$45.00/50mg
22118-09-8
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$21.21/10gm:
100-61-8
406 suppliers
$8.00/1g
29182-97-6
49 suppliers
$45.00/50mg
100-61-8
406 suppliers
$8.00/1g
29182-97-6
49 suppliers
$45.00/50mg
579-10-2
87 suppliers
$50.00/25g
29182-97-6
49 suppliers
$45.00/50mg