2-Chloro-4-(ethoxycarbonyl)benzoic acid synthesis

1synthesis methods

Product Name:2-Chloro-4-(ethoxycarbonyl)benzoic acid
CAS Number:911314-33-5
Molecular formula:C10H9ClO4
Molecular Weight:228.63

76008-74-7 Synthesis

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: N-ethyl-N,N-diisopropylamine / palladium diacetate; 1,3-bis-(diphenylphosphino)propane / dimethyl sulfoxide / 9 h / 100 °C
2: hydrogen / palladium 10% on activated carbon / tetrahydrofuran / 3 h / 20 °C

References:

EP1867639,2007,A1

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