2-cyclohexyl-1-(diaminomethylidene)guanidine synthesis
2synthesis methods
- Product Name:2-cyclohexyl-1-(diaminomethylidene)guanidine
- CAS Number:15233-32-6
- Molecular formula:C8H17N5
- Molecular Weight:183.25
Yield:-
Reaction Conditions:
with hydrogenchloride in acetonitrile at 170;
Steps:
1.4
4. Synthesis of SD-000176 and SD-000196: Aniline was dissolved in acetonitrile and then added strong hydrochloric acid by 1 equivalent. Dicyandiamide was added, a reactant was heated up to 170° C., and then a crystalline material was filtered.
References:
US2017/333370,2017,A1 Location in patent:Paragraph 0088