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2-ethynylbenzaMide synthesis

4synthesis methods
4001-73-4 Synthesis
2-BROMOBENZAMIDE

4001-73-4
162 suppliers
$8.00/1g

2-ethynylbenzaMide

1207252-50-3
8 suppliers
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: copper(l) iodide; palladium diacetate; triethylamine; triphenylphosphine / 90 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

References:

Varela-Fernandez, Alejandro;Varela, Jesus A.;Saa, Carlos [Advanced Synthesis and Catalysis,2011,vol. 353,# 11-12,p. 1933 - 1937]