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ChemicalBook CAS DataBase List 2-(FLUOROSULFONYL)DIFLUOROACETYL FLUORIDE

2-(FLUOROSULFONYL)DIFLUOROACETYL FLUORIDE synthesis

10synthesis methods
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Yield: 78%

Reaction Conditions:

Stage #1:polytetrafluoroethylene with sulfur trioxide at 40 - 60; for 48 h;
Stage #2: with triethylamine for 1 h;

References:

Thomas, Brian H.;Shafer, Gregory;Ma, Jing Ji;Tu, Ming-Hu;DesMarteau, Darryl D. [Journal of Fluorine Chemistry,2004,vol. 125,# 8,p. 1231 - 1240]

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