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(2-formylphenoxy)acetonitrile(SALTDATA: FREE) synthesis

3synthesis methods
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Yield:125418-83-9 99%

Reaction Conditions:

Stage #1: salicylaldehydewith potassium carbonate in N,N-dimethyl-formamide at 20; for 0.25 h;Schlenk technique;Inert atmosphere;
Stage #2: bromoacetonitrile in N,N-dimethyl-formamide at 20; for 4 h;

References:

Wang, Ali;Xie, Xin;Zhang, Chunli;Liu, Yuanhong [Chemical Communications,2020,vol. 56,# 99,p. 15581 - 15584] Location in patent:supporting information

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