ChemicalBook CAS DataBase List 2-Hexanone

2-Hexanone synthesis

12synthesis methods

Product Name:2-Hexanone
CAS Number:591-78-6
Molecular formula:C6H12O
Molecular Weight:100.16

MnBK can be produced by a reaction between acetic acid and ethylene under pressure MnBK can be produced by a reaction between acetic acid and ethylene under pressure.

693-02-7
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$10.00/1g

591-78-6
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$23.80/u

Yield:591-78-6 99%

Reaction Conditions:

with water;methyl(triphenylphosphine)gold(I);sulfuric acid in methanol at 70; for 1 h;

Steps:

35 Example 35
Example 35 To a solution in which 0.001 g of methyl(triphenylphosphine)gold (0.002 mmol) was dissolved in 1 ml of methanol, 0.09 g of 1-hexyne (1 mmol) and an aqueous solution in which 0.05 g of concentrated sulfuric acid (0.5 mmol) was dissolved in 0.5 ml of water were added. After stirring at 60° C. for 2 hours, the yield of 2-hexanone was 99% (catalyst turnover number: 495).

References:

Mizushima, Eiichiro;Hayashi, Teruyuki;Sato, Kazuhiko;Tanaka, Masato US2005/143597, 2005, A1 Location in patent:Page/Page column 7

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