2-IODOBENZENE-1-SULFONAMIDE, 95%+ synthesis
- Product Name:2-IODOBENZENE-1-SULFONAMIDE, 95%+
- CAS Number:53730-99-7
- Molecular formula:C6H6INO2S
- Molecular Weight:283.09
146720-72-1
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Yield:53730-99-7 86%
Reaction Conditions:
with trifluoroacetic acid at 20; for 6 h;
Steps:
A; 4
At room temperature, 4.3 g (12.68 mmol) of N-tert-butyl-2-iodobenzenesulfonamide are stirred in 15 ml of trifluoroacetic acid for 6 h. The solid obtained after evaporation of the solution is washed with water. This gives 3.1 g (86% of theory) of 2-iodobenzenesulfonamide.
References:
US2010/285964,2010,A1 Location in patent:Page/Page column 4; 5; 20
3306-62-5
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63059-25-6
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$16.00/1g
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63059-29-0
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$29.00/250mg
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88-21-1
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$12.00/25g
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