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2-IODOBENZOYLACETONITRILE synthesis

2synthesis methods
-

Yield:158387-19-0 79%

Reaction Conditions:

with sodium hydride in tetrahydrofuran;mineral oil; for 2 h;Reflux;

References:

Boelke, Andreas;Caspers, Lucien D.;Kuczmera, Thomas J.;Lork, Enno;Nachtsheim, Boris J. [Organic Letters,2020,vol. 22,# 18,p. 7261 - 7266] Location in patent:supporting information