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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List 2-Methoxybenzyl alcohol
612-16-8

2-Methoxybenzyl alcohol synthesis

11synthesis methods
Synthesis of 2-Methoxybenzyl Alcohol: Under an inert nitrogen (N₂) atmosphere, after dehydration and deoxygenation, 2-methoxybenzoic acid (76.2 mg, 0.5 mmol) was added to the reaction flask, followed by the addition of liquid borane (290 μL, 2 mmol). The reaction was carried out at room temperature for 12 hours. After completion, the mixture was removed from the glovebox, and trimethoxybenzene (84.23 mg, 0.5 mmol) was added as an internal standard. The mixture was dissolved in CDCl₃, stirred for 10 minutes, and then sampled for nuclear magnetic resonance (NMR) analysis. The yield was calculated to be 99%.
o-Anisaldehyde

135-02-4
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2-Methoxybenzyl alcohol

612-16-8
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$11.00/5g

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Yield:612-16-8 100%

Reaction Conditions:

with sodium tetrahydroborate in methanol at 20; for 1 h;

Steps:

Step-I (Preparation of benzyl alcohols)
General procedure: benzaldehyde derivatives (1 mmol) in methanol (15 mL), sodium borohydride (2 mmol) and stirred at room temperature for 1 h. Usual work-up, quantitative yield.

References:

Parihar, Swati;Kumar, Amit;Chaturvedi, Amit K.;Sachan, Naresh Kumar;Luqman, Suaib;Changkija, Bendangla;Manohar, Murli;Prakash, Om;Chanda;Khan, Feroz;Chanotiya;Shanker, Karuna;Dwivedi, Anila;Konwar, Rituraj;Negi, Arvind S. [Journal of Steroid Biochemistry and Molecular Biology,2013,vol. 137,p. 332 - 344]

FullText

579-75-9 Synthesis
o-Anisic acid

579-75-9
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2-Methoxybenzyl alcohol

612-16-8
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References
2-Methoxybenzylamine

6850-57-3
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2-Methoxybenzyl alcohol

612-16-8
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$11.00/5g

References
606-45-1 Synthesis
Methyl 2-methoxybenzoate

606-45-1
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2-Methoxybenzyl alcohol

612-16-8
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References
Benzene, 1-methoxy-2-[[(trimethylsilyl)oxy]methyl]-

195064-77-8
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2-Methoxybenzyl alcohol

612-16-8
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References

2-Methoxybenzyl alcohol Related Search:

Ethyl acetate 4-Hydroxybenzyl alcohol Benzyl alcohol Triphenylmethanol 4-Methylbenzyl alcohol Benzhydrol 3-Phenoxybenzyl alcohol 2,6-Dimethoxybenzoic acid 2,4,5-Trimethoxybenzoic acid 2,4-Dimethoxybenzoic acid