2-(METHYLTHIO)-5-(TRIBUTYLSTANNYL)PYRIMIDINE synthesis
- Product Name:2-(METHYLTHIO)-5-(TRIBUTYLSTANNYL)PYRIMIDINE
- CAS Number:120717-37-5
- Molecular formula:C17H32N2SSn
- Molecular Weight:415.22
14001-67-3
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429-41-4
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813-19-4
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120717-37-5
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Yield:120717-37-5 72%
Reaction Conditions:
bis(η3-allyl-μ-chloropalladium(II)) in tetrahydrofuran;addn. of Bu4NF in THF to mixture of pyrimidine deriv., Bu6Sn2 and Pd-catalyst (N2-stream); stirring at ambiente temp. for 4h; GLC-monitoring; addn. of EtOAc; washing (water); flash chromy. (silica; hexane/EtOAc 1:1); distn.;
References:
Sandosham, Jessie;Undheim, Kjell [Acta Chemica Scandinavica,1989,vol. 43,# 7,p. 684 - 689]
14001-67-3
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$8.00/250mg
4226-01-1
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120717-37-5
27 suppliers
$45.00/50mg