2-Pyridinamine,N,3-dimethyl-(9CI) synthesis
- Product Name:2-Pyridinamine,N,3-dimethyl-(9CI)
- CAS Number:156267-13-9
- Molecular formula:C7H10N2
- Molecular Weight:122.17
Yield:156267-13-9 64%
Reaction Conditions:
Stage #1: 3-methylpyridin-2-ylaminewith sodium hydride in tetrahydrofuran;mineral oil at 0; for 0.5 h;Inert atmosphere;Sealed tube;
Stage #2: methyl iodide in tetrahydrofuran;mineral oil at 0 - 20; for 1 h;Inert atmosphere;Sealed tube;
References:
Karmel, Caleb;Chen, Zhewei;Hartwig, John F. [Journal of the American Chemical Society,2019,vol. 141,# 17,p. 7063 - 7072] Location in patent:supporting information
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