2-(tert-Butyl)-5-nitropyriMidin-4-aMine synthesis
- Product Name:2-(tert-Butyl)-5-nitropyriMidin-4-aMine
- CAS Number:70227-51-9
- Molecular formula:C8H12N4O2
- Molecular Weight:196.21
70227-50-8
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Yield:70227-51-9 78%
Reaction Conditions:
with ammonia in methanol;water;
Steps:
3
Compound 3.4 was dissolved in MeOH (1 mL) and ammonium hydroxide solution (1.5 mL) was added. The reaction mixture was stirred overnight. After removal of excess ammonia and MeOH, the mixture was extracted with chloroform. After drying with anhydrous sodium sulfate and removal of the solvent, compound 3.5 (89 mg, ~78%) was obtained and used without further purification.
References:
WO2006/65703,2006,A1 Location in patent:Page/Page column 104
18202-73-8
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42351-88-2
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70227-49-5
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