2-tert-butylpyridin-4(1H)-one synthesis
- Product Name:2-tert-butylpyridin-4(1H)-one
- CAS Number:1163706-65-7
- Molecular formula:C9H13NO
- Molecular Weight:151.21
74628-14-1
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Yield:-
Reaction Conditions:
with ammonia in water at 80; for 18 h;
Steps:
D4
2-tert.butyl gama-pyrone, (3.02 g, prepared by the procedure of Koreeda and Akagi Tetrahedron Letters 1980, 21, 1197-1200.) is heated for 18 hours at 80° C. in 35% aqueous ammonia (50 ml). The reaction mixture is cooled to room temperature, partitioned with CH2Cl2, and the organic layer washed with water. Drying of the organic layer over magnesium sulphate followed by evaporation gives the title compound.
References:
US2009/163469,2009,A1 Location in patent:Page/Page column 38
3282-30-2
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