2-Thienylpyrrole synthesis
- Product Name:2-Thienylpyrrole
- CAS Number:52707-46-7
- Molecular formula:C8H7NS
- Molecular Weight:149.21
Yield:52707-46-7 71%
Reaction Conditions:
Stage #1: sodium pyrrolidewith zinc(II) chloride in tetrahydrofuran at 20; for 0.5 h;Inert atmosphere;
Stage #2: with tris(dibenzylideneacetone)dipalladium(0) chloroform complex;johnphos in tetrahydrofuran at 20; for 0.166667 h;Inert atmosphere;
Stage #3: 2-bromothiophene in tetrahydrofuran at 100; for 17 h;Inert atmosphere;
References:
Shimogawa, Hiroyuki;Murata, Yasujiro;Wakamiya, Atsushi [Organic Letters,2018,vol. 20,# 17,p. 5135 - 5138] Location in patent:supporting information
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52707-46-7
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