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ChemicalBook CAS DataBase List 1-tert-butyl 4-ethyl 3-oxopiperidine-1,4-dicarboxylate

1-tert-butyl 4-ethyl 3-oxopiperidine-1,4-dicarboxylate synthesis

2synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 87 percent / H2, 3M HCl / 10percent Pd/C / H2O; ethanol / 48 h / 4560 Torr
2: 99 percent / Na2CO3 / H2O; tetrahydrofuran / 0 deg C, 30 min and room t., 2 h

References:

Willert, Marianne;Bols, Mikael [Acta Chemica Scandinavica,1998,vol. 52,# 4,p. 461 - 468]