BIS[1-(2-NITROPHENYL)ETHYL] N,N-DIISOPROPYLPHOSPHORAMIDITE synthesis
- Product Name:BIS[1-(2-NITROPHENYL)ETHYL] N,N-DIISOPROPYLPHOSPHORAMIDITE
- CAS Number:207516-14-1
- Molecular formula:C22H30N3O6P
- Molecular Weight:463.46
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Yield:-
Steps:
Multi-step reaction with 2 steps
1: 89 percent / DIBAL-H / tetrahydrofuran; toluene / 0.25 h / 0 °C
2: 80 percent / Et3N / tetrahydrofuran / -20 - 20 °C
References:
Scheigetz, John;Roy, Bruno [Synthetic Communications,2000,vol. 30,# 8,p. 1437 - 1445]