3-phenyl-4H-1lambda6-pyrido[2,3-e][1,2,4]thiadiazine-1,1-dione synthesis
1synthesis methods
- Product Name:3-phenyl-4H-1lambda6-pyrido[2,3-e][1,2,4]thiadiazine-1,1-dione
- CAS Number:216507-85-6
- Molecular formula:C12H9N3O2S
- Molecular Weight:259.28
Yield:-
Steps:
Multi-step reaction with 2 steps
1: potassium hydroxide / dichloromethane; water / 8 h / 0 - 20 °C
2: potassium carbonate / N,N-dimethyl-formamide / 80 °C
References:
Cherepakha, Artem;Kovtunenko, Vladimir O.;Tolmachev, Andrey;Lukin, Oleg [Journal of Heterocyclic Chemistry,2013,vol. 50,# 5,p. 1071 - 1077]