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23360-63-6

Butanedioic acid, 2-(triphenylphosphoranylidene)-, 1,4-diethyl ester synthesis

5synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: ethyl acetate / 24.25 h / 20 °C
2: anhydrous sodium carbonate / dichloromethane; lithium hydroxide monohydrate / 0.25 h / 20 °C

References:

Liu, Teng;He, Chixian;Wang, Fan;Shen, Xiang;Li, Yongqin;Lang, Man;Li, Guijun;Huang, Chao;Cheng, Feixiang [Synthesis,2021,vol. 53,# 3,p. 518 - 526]