ChemicalBook CAS DataBase List (R)-5-(hydroxymethyl)-3-(4-iodophenyl)oxazolidin-2-one

(R)-5-(hydroxymethyl)-3-(4-iodophenyl)oxazolidin-2-one synthesis

1synthesis methods

Product Name:(R)-5-(hydroxymethyl)-3-(4-iodophenyl)oxazolidin-2-one
CAS Number:252330-13-5
Molecular formula:C10H10INO3
Molecular Weight:319.1

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(R)-5-(hydroxymethyl)-3-(4-iodophenyl)oxazolidin-2-one

252330-13-5
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: zinc perchlorate / chloroform / 24 h / 55 °C
2: sodium hydroxide / dichloromethane; water / 24 h
3: dmap; C₂₀H₁₄AlNO₃ / dichloromethane / 60 h / 25 °C / 760.05 Torr / Sealed tube

References:

Lee, Yuseop;Choi, Jonghoon;Kim, Hyunwoo [Organic Letters,2018,vol. 20,# 16,p. 5036 - 5039]

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