4,4,5,5-TETRAMETHYL-2-(4-TERT-BUTYL-1-CYCLOHEXEN-1-YL)-1,3,2-DIOXABOROLANE synthesis
- Product Name:4,4,5,5-TETRAMETHYL-2-(4-TERT-BUTYL-1-CYCLOHEXEN-1-YL)-1,3,2-DIOXABOROLANE
- CAS Number:287944-06-3
- Molecular formula:C16H29BO2
- Molecular Weight:264.21
77412-96-5
5 suppliers
inquiry
73183-34-3
593 suppliers
$6.00/5g
287944-06-3
59 suppliers
$119.00/1g
Yield:287944-06-3 94%
Reaction Conditions:
with triphenylphosphine;bis(triphenylphosphine)palladium(II) chloride in toluene;mixt. in toluene stirred at 50°C for 3 h; treated (H2O) at room temp.; extd. (benzene); washed with brine; dried (MgSO4); purified by chromy. on silica gel or by distn. (vac.);
References:
Takagi, Jun;Takahashi, Kou;Ishiyama, Tatsuo;Miyaura, Norio [Journal of the American Chemical Society,2002,vol. 124,# 27,p. 8001 - 8006]
61676-62-8
330 suppliers
$11.19/5G
41780-53-4
10 suppliers
inquiry
287944-06-3
59 suppliers
$119.00/1g
77412-96-5
5 suppliers
inquiry
25015-63-8
224 suppliers
$22.39/5G
287944-06-3
59 suppliers
$119.00/1g
98-53-3
278 suppliers
$5.00/1g
287944-06-3
59 suppliers
$119.00/1g