3-(2-Bromophenyl)-5-phenyl-1,2,4-oxadiazole synthesis
- Product Name:3-(2-Bromophenyl)-5-phenyl-1,2,4-oxadiazole
- CAS Number:827332-78-5
- Molecular formula:C14H9BrN2O
- Molecular Weight:301.14
6630-33-7
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Yield:-
Steps:
Multi-step reaction with 4 steps
1: hydroxylamine hydrochloride; sodium acetate / ethanol
2: N-chloro-succinimide / N,N-dimethyl-formamide / 4 h / 20 °C / Inert atmosphere
3: triethylamine / N,N-dimethyl-formamide / 6 h / 0 - 20 °C / Inert atmosphere
4: potassium phosphate; oxygen / N,N-dimethyl-formamide / 10 h / 60 °C / 760.05 Torr
References:
Zhang, Feng-Lian;Wang, Yi-Feng;Chiba, Shunsuke [Organic and Biomolecular Chemistry,2013,vol. 11,# 36,p. 6003 - 6007]
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1000210-73-0
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2042-37-7
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55-21-0
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38435-47-1
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827332-78-5
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