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154257-70-2

3-(3,4-DIMETHOXYPHENYL)PYRAZOLE synthesis

6synthesis methods
127172-22-9 Synthesis
1-(3,4-diMethoxyphenyl)-3-(diMethylaMino)prop-2-en-1-one

127172-22-9
24 suppliers
$85.00/250mg

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Yield:154257-70-2 75%

Reaction Conditions:

with hydrazine hydrate in ethanol; for 3 h;Reflux;

Steps:

2.3. Synthesis of Pyrazoles (P1-P11)

General procedure: A mixture of enaminone(0.01 mol) and hydrazine hydrate 99% (0.01 mol) wasreAuxed in absolute alcohol for 3 hours. +e mixture waspoured into cold water. +e precipitate was obtained. +eproduct was obtained by 6ltration under vacuum. +eproduct was recrystallized from ethanol [25].

References:

Bhat, Mashooq Ahmad;Al-Omar, Mohamed A.;Naglah, Ahmed M.;Khan, Abdul Arif;Bonomo, Maria Grazia [Journal of Chemistry,2019,vol. 2019,art. no. 2467970]