3-(4-FLUORO-PHENYL)-3-FURAN-2-YL-PROPYLAMINE synthesis
- Product Name:3-(4-FLUORO-PHENYL)-3-FURAN-2-YL-PROPYLAMINE
- CAS Number:380878-55-7
- Molecular formula:C13H14FNO
- Molecular Weight:219.25
456-22-4
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380878-55-7
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 80 percent / tris(4-methoxyphenyl)phosphine; dimethylcarbonate / Pd(OAc)2 / H2O; tetrahydrofuran / 24 h / 40 °C
2: 86 percent / NaH / tetrahydrofuran / 15 h / 0 - 20 °C
3: 36 percent / H2; cc.HCl / Pd/C / methanol / 15 h / 20 °C / 2250.18 - 3000.24 Torr
References:
Martyres, Domnic;Schmiedt, Frank [Tetrahedron Letters,2006,vol. 47,# 10,p. 1649 - 1651]
879218-23-2
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374918-00-0
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15817-51-3
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23973-22-0
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380878-55-7
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