
3,5'-Di-O-acetyl-2'-deoxyuridine synthesis
- Product Name:3,5'-Di-O-acetyl-2'-deoxyuridine
- CAS Number:13030-62-1
- Molecular formula:C13H16N2O7
- Molecular Weight:312.28

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23197-88-8
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13030-62-1
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Yield:13030-62-1 96%
Reaction Conditions:
with O-(3-sulfopropyl)-functionalized nano γ-Al2O3 in neat (no solvent) at 20 - 50; for 0.5 h;
Steps:
1.4 Typical procedure for the preparation of 2c
General procedure: To a stirred suspension of d-glucose (1 mmol) in acetic anhydride (5.1 mmol) at room temperature was added sulfonic acid functionalized nano γ-Al2O3 (50 mg). The mixture was stirred at 50 °C for 40 min. After completion of the reaction (TLC), the mixture was put into diethyl ether (50 mL) and microporous filtration (microporous membrane: PVDF, pore sizes: 0.1 μm). The solvents were removed under reduced pressure and the crude product was passed through a short pad of silica to give pure acetylated product 2c. The catalyst was washed with absolute EtOH, dried and re-used for a consecutive run under the same reaction conditions.
References:
Wu, Liqiang;Yin, Zhikui [Carbohydrate Research,2013,vol. 365,p. 14 - 19]

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13030-62-1
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13030-62-1
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13030-62-1
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50-89-5
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13030-62-1
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$125.00/250mg