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ChemicalBook CAS DataBase List 3,5-DIBROMO-4-METHYLANILINE
13194-73-5

3,5-DIBROMO-4-METHYLANILINE synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 60 percent / Br2; Fe / CHCl3 / 24 h / 50 °C
2: 75 percent / Na2S2O4 / 2-methoxy-ethanol; H2O / 3 h / 110 °C

References:

Iwasaki, Tomokazu;Kohinata, Yusaku;Nishide, Hiroyuki [Organic Letters,2005,vol. 7,# 5,p. 755 - 758]

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