ChemicalBook CAS DataBase List 3,5-DIMETHOXYBENZYL BROMIDE

3,5-DIMETHOXYBENZYL BROMIDE synthesis

9synthesis methods

Product Name:3,5-DIMETHOXYBENZYL BROMIDE
CAS Number:877-88-3
Molecular formula:C9H11BrO2
Molecular Weight:231.09

705-76-0
307 suppliers
$10.00/1g

877-88-3
223 suppliers
$5.00/250mg

Yield:877-88-3 100%

Reaction Conditions:

with phosphorus tribromide in benzene at 20;

Steps:

Step-II (Preparation of benzyl bromides)

General procedure: benzyl alcohols (1 mmol) in dry benzene (15 mL) and phosphorus tribromides (0.5 mL) and stirred at room temperature to get respective benzyl bromides in quantitative yields, usual work-up.

References:

Parihar, Swati;Kumar, Amit;Chaturvedi, Amit K.;Sachan, Naresh Kumar;Luqman, Suaib;Changkija, Bendangla;Manohar, Murli;Prakash, Om;Chanda;Khan, Feroz;Chanotiya;Shanker, Karuna;Dwivedi, Anila;Konwar, Rituraj;Negi, Arvind S. [Journal of Steroid Biochemistry and Molecular Biology,2013,vol. 137,p. 332 - 344]