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ChemicalBook CAS DataBase List 3,5-Dimethylbenzotrifluoride
86845-29-6

3,5-Dimethylbenzotrifluoride synthesis

10synthesis methods
22445-41-6 Synthesis
1-Iodo-3,5-dimethylbenzene

22445-41-6
207 suppliers
$5.00/5g

81290-20-2 Synthesis
(Trifluoromethyl)trimethylsilane

81290-20-2
420 suppliers
$13.00/1g

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Yield:86845-29-6 76%

Reaction Conditions:

with copper(l) iodide;silver fluoride;sodium t-butanolate;N,N`-dimethylethylenediamine in 1-methyl-pyrrolidin-2-one at 20 - 90; for 5.5 h;Inert atmosphere;

References:

Weng, Zhiqiang;Lee, Richmond;Jia, Weiguo;Yuan, Yaofeng;Wang, Wenfeng;Feng, Xue;Huang, Kuo-Wei [Organometallics,2011,vol. 30,# 11,p. 3229 - 3232] Location in patent:experimental part