3,6-Dibromo-benzo[b]thiophene synthesis
- Product Name:3,6-Dibromo-benzo[b]thiophene
- CAS Number:1426082-37-2
- Molecular formula:C8H4Br2S
- Molecular Weight:291.99
28560-56-7
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1426082-37-2
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Yield:1426082-37-2 98%
Reaction Conditions:
Stage #1: 2,3,6-tribromobenzo[b]thiophenewith n-butyllithium in tetrahydrofuran;hexane at -78; for 0.5 h;Inert atmosphere;
Stage #2: with methanol in tetrahydrofuran;hexane; for 0.0833333 h;Inert atmosphere;
References:
Berens, Henning R. V.;Mohammad, Kausar;Reiss, Guido J.;Müller, Thomas J. J. [Journal of Organic Chemistry,2021,vol. 86,# 12,p. 8000 - 8014] Location in patent:supporting information
![6-BROMO-BENZO[B]THIOPHENE](/CAS/GIF/17347-32-9.gif)
17347-32-9
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$7.00/250mg
1426082-37-2
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57848-46-1
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$9.00/1g
1426082-37-2
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![6-BROMO-BENZO[B]THIOPHENE-2-CARBOXYLIC ACID](/CAS/GIF/19075-58-2.gif)
19075-58-2
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$39.00/500mg
1426082-37-2
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105191-64-8
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$55.00/250mg
1426082-37-2
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