(3-(Benzyloxy)phenyl)methanamine hydrochloride synthesis
- Product Name:(3-(Benzyloxy)phenyl)methanamine hydrochloride
- CAS Number:104566-41-8
- Molecular formula:C14H16ClNO
- Molecular Weight:249.74
104566-43-0
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104566-41-8
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Yield:104566-41-8 79%
Reaction Conditions:
with hydrogenchloride in dichloromethane at 20; for 1 h;
Steps:
R.D.1.3 Synthesis of 3-(benzyloxy)benzylaminehydrochloride (D-1)
To the compound (1.6 g, 7.6 mmol) obtained in step 204 2 was added 3 mol/L 206 hydrogen chloride(dichloromethane solution, 5 mL), and the mixture was stirred at room temperature for 1 hr, and concentratedunder reduced pressure to give the 207 title compound ( 1.5 g , 6.0 mmol, 79%). MS(ESI) m/z 214 (M+H)+ 1H NMR (400 MHz, CD3OD): δ7.47-7.30 (m, 6H), 7.09 (s, 1H), 7.01-6.99 (m, 2H), 5.12 (s, 2H), 3.95 (s,2H) .
References:
US2016/332999,2016,A1 Location in patent:Paragraph 0407; 0408; 0409
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104566-41-8
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104566-41-8
27 suppliers
$119.00/250mg