3-BORONO-2-METHOXYBENZOIC ACID synthesis
- Product Name:3-BORONO-2-METHOXYBENZOIC ACID
- CAS Number:913836-10-9
- Molecular formula:C8H9BO5
- Molecular Weight:195.97
124-38-9
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38603-09-7
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$25.00/1g
913836-10-9
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$104.00/250mg
Yield: 72%
Reaction Conditions:
Stage #1:2,6-dibromoanisole with n-butyllithium in diethyl ether;hexane at -80; for 0.5 h;Inert atmosphere;
Stage #2: with Triisopropyl borate in tetrahydrofuran;diethyl ether;hexane at -70; for 0.5 h;Inert atmosphere;
Stage #3:carbon dioxideFurther stages;
References:
Kurach, Pawel;Lulinski, Sergiusz;Serwatowski, Janusz [European Journal of Organic Chemistry,2008,# 18,p. 3171 - 3178] Location in patent:experimental part