3-BUTENAMIDE synthesis
- Product Name:3-BUTENAMIDE
- CAS Number:28446-58-4
- Molecular formula:C4H7NO
- Molecular Weight:85.1
109-75-1
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28446-58-4
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Yield: 100%
Reaction Conditions:
with Acetaldehyde oxime in methanol at 65; for 4 h;
Steps:
General procedure: A typical reaction was carried out in a 10 mL flask. Benzonitrile (2 mmol), CuII-4 Å (0.2 g), acetaldoxime (6 mmol) and MeOH (4 mL) were stirred at 65 °C for 4 h. The solid was filtered, washed with MeOH and the filtrate evaporated. The residue was subjected to GC-MS analysis and NMR spectroscopy. The filtered catalyst can be recycled after drying at about 150 °C for 1 h.
References:
Kiss, Árpád;Hell, Zoltán [Tetrahedron Letters,2011,vol. 52,# 45,p. 6021 - 6023] Location in patent:experimental part
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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28446-58-4
28 suppliers
$109.90/5 mg
625-38-7
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$25.00/5g
28446-58-4
28 suppliers
$109.90/5 mg
109-75-1
160 suppliers
$9.00/1g
625-38-7
172 suppliers
$25.00/5g
28446-58-4
28 suppliers
$109.90/5 mg
1470-91-3
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28446-58-4
28 suppliers
$109.90/5 mg