3-Chloro-5-(3,5-dimethylphenyl)phenol synthesis
- Product Name:3-Chloro-5-(3,5-dimethylphenyl)phenol
- CAS Number:1261942-01-1
- Molecular formula:C14H13ClO
- Molecular Weight:232.71
Yield:1261942-01-1 69%
Reaction Conditions:
Stage #1: 3-monochlorophenolwith potassium hydroxide in toluene at 50; for 0.166667 h;
Stage #2: with carbon dioxide at 190; under 19001.3 Torr; for 2 h;Inert atmosphere;Autoclave;
Stage #3: 3,5-dimethylphenyl iodidewith palladium diacetate;acetic acid;silver carbonate at 130; under 19001.3 Torr; for 40 h;Inert atmosphere;Autoclave;regioselective reaction;Reagent/catalyst;
References:
Luo, Junfei;Preciado, Sara;Larrosa, Igor [Journal of the American Chemical Society,2014,vol. 136,# 11,p. 4109 - 4112] Location in patent:supporting information
2420-26-0
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22445-41-6
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1261942-01-1
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