
3-Cyclohexyl-1H-indole synthesis
- Product Name:3-Cyclohexyl-1H-indole
- CAS Number:100717-32-6
- Molecular formula:C14H17N
- Molecular Weight:199.29
![Phosphonic acid, [hydroxy(2-nitrophenyl)methyl]-, diethyl ester](/CAS/20180601/GIF/79202-15-6.gif)
79202-15-6
0 suppliers
inquiry

100717-32-6
34 suppliers
inquiry
Yield:-
Steps:
Multi-step reaction with 5 steps
1.1: 97 percent / H2 / 10 percent Pd/C / ethanol / 72 h / 100 °C / 38786.1 Torr
2.1: 57 percent / aq. KOH; BnEt3NCl / CH2Cl2 / Heating
3.1: LDA / tetrahydrofuran; hexane / 0.5 h / -78 °C
3.2: 73 percent / HMPA / tetrahydrofuran; hexane / -78 - 20 °C
4.1: AIBN / acetonitrile / 0.25 h / 100 °C
5.1: Raney-Ni / ethanol
References:
Tokuyama;Watanabe;Hayashi;Kurokawa;Peng;Fukuyama [Synlett,2001,# 9,p. 1403 - 1406]
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
0 suppliers
inquiry

100717-32-6
34 suppliers
inquiry