3-DEOXY-3-FLUORO-D-GLUCOSE synthesis
- Product Name:3-DEOXY-3-FLUORO-D-GLUCOSE
- CAS Number:14049-03-7
- Molecular formula:C6H11FO5
- Molecular Weight:182.15
2595-05-3
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14049-03-7
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: pyridine / dichloromethane / 1.5 h / -20 °C
2: cesium fluoride / tert-butyl alcohol / 26 h / 80 °C
3: Dowex 50W X8, H+ / water; 1,4-dioxane / 18 h / 65 °C
References:
Liu, Zilei;Jenkinson, Sarah F.;Vermaas, Tom;Adachi, Isao;Wormald, Mark R.;Hata, Yukako;Kurashima, Yukiko;Kaji, Akira;Yu, Chu-Yi;Kato, Atsushi;Fleet, George W. J. [Journal of Organic Chemistry,2015,vol. 80,# 9,p. 4244 - 4258]
![(3aR,6S,6aS)-5-((S)-2,2-dimethyl-1,3-dioxolan-4-yl)-6-fluoro-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxole](/CAS/20211123/GIF/14049-05-9.gif)
14049-05-9
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14049-03-7
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55951-90-1
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14049-03-7
69 suppliers
$45.00/10 mg